boron trifluoride

(redirected from Boron trifluoride etherate)
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a pungent colorless gas

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The reaction of pyrrolomethane 1 with 3- (phenylthio)propanal 3 in the presence of ytterbium (III) trifluoromethan- esulfonate hydrate in catalytic amount gave the 5-(2- thiophenyl ethane)-1,9-dimethyldipyrromethane 4, which was treated with DDQ and boron trifluoride etherate in the presence of triethylamine yielded 8-(2- thiophenylethan) 4,4-difluoro-3,5dimethyl-4-bora-3a,4a-diaza-3-indacene 5.