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2], a piece of platinum sheet as a counter electrode, and the saturated calomel electrode as a reference electrode.
In this electrochemical 3-electrodes system, the embedded rebar acts as working electrode, stainless steel plate acts as counter electrode and the saturated calomel electrode acts as reference electrode.
a saturated calomel electrode in a pH 12 sodium hydroxide solution.
The electrochemical cell of 500 ml capacity fitted with saturated calomel electrode (SCE) as reference electrode, platinum foil as auxillary electrode and 316L SS as working electrode was used for all measurements.
Cyclic voltammogram (CV) of the sample was carried out in a three-electrode cell (PANI as a working electrode, Pt-foiled as a counter electrode, and saturated calomel electrode (SCE) as a reference electrode) using a CHI660A electrochemical workstation (CH Instrument, CN).
All Experiments were carried out using a three electrode cell with saturated calomel electrode (SCE) and platinum electrode as reference and counter electrode respectively.
The electrobath used in the electrolysis test consisted of a conductive, coated electrode (the working electrode), a platinum electrode (the counter electrode), and a saturated calomel electrode (the reference electrode), and is depicted in Fig.